Introducing the much-heralded new book that explains this revolutionary new analytical sample preparation procedure. Provides a theoretical basis for understanding microwave acid sampling requiring elemental or chemical analysis. Describes techniques and equipment found most effective. Gives direct practical applications of the methods to a variety of sample types. Covers most aspects of closed vessel microwave digestion and open vessel acid composition. Demonstrates fundamental relationships that can be used to predict the conditions that will occur under specific parameter settings. Addresses safety considerations for each technique demonstrated. This
book is truly multidisciplinary: its techniques can be used in inorganic elemental analysis, sample digestion, food analysis, environmental sample preparation chemistry, and other areas.
Readership: Chemistry graduates and researchers working in inorganic elemental analysis, sample digestion, food analysis, environmental sample preparation chemistry, and related areas.
Introduction to Microwave Acid Decomposition
Microwave Heating: Theoretical Concepts and Equipment Design
Guidelines for Developing Microwave Dissolution Methods for Geological and Metallurgical Samples
Open Reflux Vessels for Microwave Digestion: Botanical, Biological, and Food Samples for Elemental Analysis by Automated FIA/ICP
Applications of Microwave Digestion in the Pharmaceutical Industry
Monitoring and Predicting Temperature and Pressure in Microwave Dissolution
Microwave Digestion of Biological Samples for Selenium Analysis by Electrothermal Atomic Absorption Spectrometry
Kjeldahl Nitrogen Determination Using a Microwave System
Remote Operation of Microwave Systems: for Solids Content Analysis and Chemical Dissolution in Highly Radioactive Environments
Manual and Robotically Controlled Microwave Pressure Dissolution of Minerals
Safety Guidelines for Microwave Systems in the Analytical Laboratory